Because of the coronavirus outbreak, some services are limited.  Facility managers have been communicating details to users as reopening plans are slowly put in place.  Please do not assume that you may use any instrument until you have been told that the instrument is available.  Contact the relevant manager if you have any questions.  Please see the MC2 coronavirus page, the Chemistry Department coronavirus page, or the McGill coronavirus webpage for more information.

av400

Liquids NMR: Bruker AVIIIHD 400 MHz NMR Spectrometer


Contact: nmr.chemistry [at] mcgill.ca (Robin Stein) - Location: OM34

Use the McGill NMR booking system to book time

DocumentationTraining - Rates


Applications

Quick 1H, 19F, 31P and 2D; 13C for concentrated samples during day and for all samples overnight; other nuclei; high temperature and low temperature work

Console

Bruker AVIIIHD (two-channel, VT, z gradient)

Probes

BBFO+ SmartProbe: tuned simultaneously to 1H and to any nucleus desired between 109Ag and 19F (for example, 13C, 31P, 15N, 11B, 29Si, etc.); has ATMA (autotune) to switch between nuclei automatically

Backup probe for 1H and 13C work

Booking rules

  • Day (9 AM-8 PM, including weekends): one hour at a time, with same day sign up; two hours total per user
  • Overnight: unlimited (sign up same day)
  • Weekends: 12 hours per user (sign up beginning Friday)

Notes

  • This spectrometer is a good choice for overnight 13C experiments

  • The spectrometer can be used for high temperature (up to +150 °C) and low temperature (down to –150 °C) experiments. Training and/or supervision are required for such work

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